中国中药杂志

2002, (11)

[打印本页] [关闭]
本期目录(Current Issue) | 过刊浏览(Past Issue) | 高级检索(Advanced Search)

枳实导滞浓缩丸质量标准研究
Studies on Quality Control Standard of Zhishidaozhi Tabloid Pills

刘友平,宋英,秦春梅,张家明
LIU You-ping1, SONG Ying2, QIN Chun-mei1, ZHANG Jia-ming2 (1.Chengdu University of TCM, Chengdu 610075, Sichuan, China; 2.The Affiliated Hospital of Chengdu University of TCM,Chengdu 610075, Sichuan, China)

摘要(Abstract):

目的 :建立枳实导滞浓缩丸的质量标准。方法 :采用TLC对处方中的大黄、枳实、黄连、黄芩进行定性鉴别 ;用HPLC法测定方中君药大黄中大黄素的含量。结果 :在TLC色谱中 ,能检出大黄、枳实、黄连、黄芩 ;大黄素在 0 .0 6 12~ 0 .6 12 0 μg与峰面积积分值呈良好的线性关系 ,r =0 .9999,平均回收率 97.9% ,RSD =2 .1%。结论 :所建立的方法对方中 4味药材能准确、快速地进行定性、定量检测 ,可用于枳实导滞浓缩丸的质量控制。
Objective:To develop the quality control standard of Zhishidaozhi Tabloid Pills. Method: Applying TLC to indentify Radix et Rhizoma Rhei,Fructus Aurantii Immaturus,Rhizoma Coptidis ,Radix Scutellariae ,and HPLC to determine the content of emodin of Radix et Rhizoma Rhei. Result:Radix et Rhizoma Rhei ,Fructus Aurantii Immaturus,Rhizoma Coptidis and Radix Scutellariae could be indentified by TLC. Emodin showed a good linear relationship at a rang of 0.0612~0.612 μg, r=0.9999. The average recovery was 97.9 %, and RSD was 2.1%. Conclusion:The methods are accurate and quick ,and can be used for the quality control of Zhishidaozhi Tabloid Pills.

关键词(KeyWords): 枳实导滞浓缩丸;TLC;HPLC;大黄素
Zhishidaozhi Tabloid Pills ; TLC; HPLC;emodin

Abstract:

Keywords:

基金项目(Foundation):

作者(Author): 刘友平,宋英,秦春梅,张家明
LIU You-ping1, SONG Ying2, QIN Chun-mei1, ZHANG Jia-ming2 (1.Chengdu University of TCM, Chengdu 610075, Sichuan, China; 2.The Affiliated Hospital of Chengdu University of TCM,Chengdu 610075, Sichuan, China)

Email:

DOI:

扩展功能
本文信息
服务与反馈
本文关键词相关文章
本文作者相关文章
中国知网
分享