中国中药杂志

2013, v.38(10) 1543-1547

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新疆藁本化学成分的研究
Chemical constituents of Conioselinum vaginatum

李兴博;齐耀东;刘海涛;张进;张昭;张本刚;
LI Xing-bo,QI Yao-dong,LIU Hai-tao,ZHANG Jin,ZHANG Zhao,ZHANG Ben-gang(Key Laboratory of Bioactive Substance and Resources Utilization of Chinese Herbal Medicine,Ministry of Education, Institute of Medicinal Plant Development,Chinese Academy of Medical Sciences, Peking Union Medical College,Beijing 100193,China)

摘要(Abstract):

采用硅胶柱色谱、凝胶柱色谱、重结晶等方法从新疆藁本中分离得到16个化合物,根据化合物的理化性质和波谱学数据分别鉴定为:藁本内酯(1),1,3-二亚油酸甘油酯(2),松柏醛(3),肉豆蔻醚(4),豆甾醇(5),β-谷甾醇(6),香草醛(7),孕烯醇酮(8),佛手柑内酯(9),花椒毒素(10),吲哚-3-甲酸甲酯(11),阿魏酸(12),(E)-3-甲氧基-4,5-亚甲二氧基肉桂醇(13),对羟基苯甲醛(14),3-甲氧基-4,5-亚甲二氧基-乙酰苯(15),α-乙氧甲基-4-羟基-苄醇(16)。化合物15为新的天然产物,化合物2,3,10,11,14,16为首次从该属植物中分离得到。
Sixteen compounds were isolated from Conioselinum vaginatum by silica column chromatography over silica gel and Sephadex LH-20,as well as recrystallization.On the basis of their physical and chemical properties and spectral data,their structures were identified as ligustilide(1),1,3-dilinolein(2),coniferaldehyde(3),myristicin(4),stigmasterol(5),β-sitosterol(6),vanillin(7),pregnenolone(8),bergapten(9),xanthotoxin(10),methyl indole-3-carboxylate(11),ferulic acid(12),(E)-3-methoxy-4,5-methylenedioxy-cinnamic alcohol(13),p-hydroxybenzaldehyde(14),3-methoxy-4,5-methylenedioxy-acetophenone(15),and α-(ethoxymethyl)-4-hydroxy-benzenemethanol(16).Among them,compound 15 was a new natural product,and compounds 2,3,10,11,14,and 16 were obtained from this genus for the first time.

关键词(KeyWords): 山芎属;新疆藁本;化学成分
Conioselinum;Conioselinum vaginatum;chemical constituents

Abstract:

Keywords:

基金项目(Foundation): 国家自然科学基金青年基金项目(81001609)

作者(Authors): 李兴博;齐耀东;刘海涛;张进;张昭;张本刚;
LI Xing-bo,QI Yao-dong,LIU Hai-tao,ZHANG Jin,ZHANG Zhao,ZHANG Ben-gang(Key Laboratory of Bioactive Substance and Resources Utilization of Chinese Herbal Medicine,Ministry of Education, Institute of Medicinal Plant Development,Chinese Academy of Medical Sciences, Peking Union Medical College,Beijing 100193,China)

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