广西血竭石油醚和醋酸乙酯部位中的化学成分(Ⅱ)Constituents in Petroleum Ether and Ethyl Acetate Extract Fractions of Dracaena cochinensis (Lour.)S.C.Chen
韦宏,文东旭,刘晓松,唐人九
Wei Hong,Wen Dongxu,Liu Xiaosong and Tang Renjiu. (Guangxi Institute of Traditional Chinese Medicine and Pharmacy,Nanning 530022)
摘要(Abstract):
目的:对广西血竭的化学成分进行研究。方法:采用溶剂提取、柱层析、薄层层析和高效液相色谱法进行分离,光谱数据鉴定化合物结构。结果:从石油醚和醋酸乙酯部位中得到10个化合物,为正二十七烷、4甲基7烯胆烷醇、阿魏酸二十二酯、阿魏酸二十四酯、阿魏酸二十六酯、阿魏酸二十八酯、紫檀、邻苯二甲酸二(2乙基)己酯、邻苯二甲酸丁酯异丁酯和4′甲氧基3′,7二羟基黄酮。结论:均为首次从广西血竭中分离得到。
Objective:To study the chemical constituents of Dracaena cochinensis.Methods:Compounds were separa ted by solvent extraction,column chromatography,TLC and HPLC,and their structures were determined by spectral ana lysis.Results:Ten compounds were isolated from the petroleum ether and ethyl acetate fractions of D.cochinensis and identified as n heptacosane,lophenol,docosanyl ferulate,tetracosanyl ferulate,hexacosanyl ferulate ,octacosanyl ferulate,pterostilbene,dioctyl phthalate,butyl isobutyl phthalate and 4' methoxy 3',7 dihydroxy flavone.Conclusion:All the compounds were isolated from this plant for the first time.
关键词(KeyWords):
广西血竭,阿魏酸酯,邻苯二甲酸酯,4'-甲氧基-3'.7-二羟基黄酮
Dracaena cochinensis;ferulic acid esters;phthalic acid esters;4' methoxy 3',7 dihydroxy flavone
基金项目(Foundation): 国家自然科学基金
作者(Author):
韦宏,文东旭,刘晓松,唐人九
Wei Hong,Wen Dongxu,Liu Xiaosong and Tang Renjiu. (Guangxi Institute of Traditional Chinese Medicine and Pharmacy,Nanning 530022)
- 广西血竭,阿魏酸酯,邻苯二甲酸酯,4'-甲氧基-3'.7-二羟基黄酮
Dracaena cochinensis - ferulic acid esters
- phthalic acid esters
- 4' methoxy 3',7 dihydroxy flavone
- 韦宏
- 文东旭
- 刘晓松
- 唐人九
Wei Hong - Wen Dongxu
- Liu Xiaosong and Tang Renjiu. (Guangxi Institute of Traditional Chinese Medicine and Pharmacy
- Nanning 530022)
- 韦宏
- 文东旭
- 刘晓松
- 唐人九
Wei Hong - Wen Dongxu
- Liu Xiaosong and Tang Renjiu. (Guangxi Institute of Traditional Chinese Medicine and Pharmacy
- Nanning 530022)