中国中药杂志

2001, (06)

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山丹芍药汤化学成分的分离与鉴定(Ⅰ)
Isolation and Elucidation of Chemical Constituents of Shandanshaoyao Decoction(Ⅰ)

文志明,徐礼燊
WEN Zhi ming,XU Li xin (Institute of Materia Medica, Chinese Academy of Medical Sciences and Peking Union Medical College, Beijing 100050,China)

摘要(Abstract):

目的 :对山丹芍药汤化学成分进行研究。方法 :水提醇沉法制备样品 ,氯仿、乙酸乙酯和水饱和正丁醇提取 ,硅胶、聚酰胺柱进行分离 ,物理、化学和光谱学方法鉴定化合物。结果和结论 :从氯仿和乙酸乙酯提取部分分得 6个化合物 ,为丹参酮ⅡA、苯甲酸、阿魏酸、隐丹参酮、β 谷甾醇和熊果酸。
Objective:To study the chemical constituents of Shandanshaoyao Decoction.Method:The sample was prepared using boiling water, then precipitated by 75% ethanol. The ethanol soluble fraction was extracted by chloroform, ethyl acetate and n butanol respectively. The extracts were isolated using silica gel and polyamide column chromatography, and the chemical constituents were identified by chemical and spectroscopic methods.Result:Six compounds were isolated from the chloroform and ethyl acetate extracts, and elucidated as tanshinone Ⅱ A, benzoic acid, ferulic acid,cryptotanshinone,β stitosterol and ursolic acid respectively.Conclusion:A preliminary study on the chemical constituents in traditional Chinese compound recipe Shandanshaoyao Decoction is reported.

关键词(KeyWords): 山丹芍药汤;化学成分
Shandanshaoyao Decoction; chemical constituents

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作者(Author): 文志明,徐礼燊
WEN Zhi ming,XU Li xin (Institute of Materia Medica, Chinese Academy of Medical Sciences and Peking Union Medical College, Beijing 100050,China)

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