中国中药杂志

2007, (22) 2357-2359

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蜘蛛香药材质量标准研究
Study on quality specification of Rhizoma et Radix Valeriana Jatamansi

狄宏晔;石晋丽;闫兴丽;赵仁;刘勇;肖培根;
DI Hong-ye1,SHI Jin-li1,YAN Xing-li1,ZHAO Ren2,LIU Yong1,XIAO Pei-gen1(1.Beijing University of Chinese Medicine,Beijing 100102,China;2.Yunnan Institute of Pharmaceuticals,Kunming 650111,China)

摘要(Abstract):

目的:制定蜘蛛香药材质量标准,为药用植物资源的开发利用提供科学依据。方法:生药学研究,浸出物测定法,灰分测定法,水分测定法,薄层色谱法及HPLC色谱法。结果:对蜘蛛香的性状、显微特征进行了描述;对15个不同产地及收集时间蜘蛛香的浸出物、总灰分、酸不溶灰分和水分进行了测定;同时对其活性成分缬草素和乙酰缬草素进行了薄层定性鉴别和HPLC定量研究。结论:通过研究制定了蜘蛛香的质量控制标准。
Objective: To provide scientific basis for the utilization and development of Valeriana jatamansi by setting up the quality control specification of V.jatamansi.Method: The pharmacognostical methods were applied.The extract of V.jatamansi was examined.Moisture and ash were determined.And the bioactive constituents were analyzed by TLC and HPLC.Result: The morphological and histological characters of V.jatamansi were observed.Content of total ash,acid-insoluble ash,and moisture of 15 samples from different habitats and times were determined.The qualitative and quantitative analysis of valtrate and acevaltrate by TLC and HPLC were preformed respectively.Conclusion: The established method can be used for the quality control of V.jatamans.

关键词(KeyWords): 蜘蛛香;质量标准;缬草素;乙酰缬草素;TLC;HPLC
Valeriana jatamansi;quality specification;valtrate;acevaltrate;TLC;HPLC

Abstract:

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基金项目(Foundation): 国家自然科学基金项目(30572463)

作者(Author): 狄宏晔;石晋丽;闫兴丽;赵仁;刘勇;肖培根;
DI Hong-ye1,SHI Jin-li1,YAN Xing-li1,ZHAO Ren2,LIU Yong1,XIAO Pei-gen1(1.Beijing University of Chinese Medicine,Beijing 100102,China;2.Yunnan Institute of Pharmaceuticals,Kunming 650111,China)

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