中国中药杂志

2010, v.35(03) 305-307

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灵猫香解毒丸的质量标准研究
Study on quality standards for Lingmaoxiang Jiedu pills

郑成;郑彬彬;姚彤炜;
ZHENG Cheng1,2,ZHENG Binbin3,YAO Tongwei1 (1. College of Pharmaceutical Sciences; Zhejiang University,Hangzhou 310080,China; 2.Zhejiang Institute for Food and Drug control,Hangzhou 310004,China; 3.Zhejiang Sencond Affiliated Hospital of Wenzhou Medical College,Wenzhou 325000,China)

摘要(Abstract):

目的:制定灵猫香解毒丸的含量测定标准。方法:采用反相高效液相色谱法测定蟾酥中华蟾酥毒基和酯蟾毒配基。结果:华蟾酥毒基和酯蟾毒配基分别在48.84~784.44,50.28~804.48ng与峰面积呈良好线性关系,平均回收率100.5%,100.3%。结论:本实验定量方法简便、实用,重复性好,能够较好控制灵猫香解毒丸的质量。
Objective:To establish the quality standards of Linmaoxiang Jiedu pills. Method:Cinobufagin and bufogenin were determined by HPLC simultaneously. Result:The average recoverys of Cinobufagin and bufogenin was 100.5% and 100.3%,their linear range were 48.74-731.10 ng and 49.90-748.50 ng,respectively. Conclusion:The method for quantification is reproducible and realizable. The method can be used to coutrol quality of Linmaoxiang Jiedu pills as the quality standards.

关键词(KeyWords): 灵猫香解毒丸;华蟾酥毒基;酯蟾毒配基;高效液相色谱
Lingmaoxiang Tiedu pills; cinobufagin; bufogenin; HPLC

Abstract:

Keywords:

基金项目(Foundation):

作者(Authors): 郑成;郑彬彬;姚彤炜;
ZHENG Cheng1,2,ZHENG Binbin3,YAO Tongwei1 (1. College of Pharmaceutical Sciences; Zhejiang University,Hangzhou 310080,China; 2.Zhejiang Institute for Food and Drug control,Hangzhou 310004,China; 3.Zhejiang Sencond Affiliated Hospital of Wenzhou Medical College,Wenzhou 325000,China)

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